BL-5A X-ray Beamline for High-throughput Macromolecular Crystallography
BL-5A is deigned for high-throughput MAD experiments with high-flux beam and a rapid data acquisition system. The wide active area of the CCD detector is particularly suited for measurements of crystals with large unit cell dimensions. A high-precision sample axis allows experiments with micro-crystals. A robot for sample exchange will be installed to improve the efficiency of experiments.
SCHEMATIC VIEW OF THE BEAMLINE
Area of Research
Macromolecular crystallography
Light Source
Multipole Wiggler
Optics
Collimating Mirror: 14.5 m
Rhodium coated silicon single crystal (Flat shaped, 1000 mm (L) x 80 mm (W) x 70 mm (T) ) with 3.5 mrad glancing angle.
Mono-chromator: 16.5 m
Numerical link type Si(111) double crystal monochromator, direct water cooling using micro-channel (1st crystal), indirect water cooling (2nd crystal)
Focusing Mirror: 18.7 m
Rhodium coated silicon single crystal (Troidal, 1000 mm (L) x 100 mm (W) x 60 mm (T) ) with 3.5 mrad glancing angle.
Photons at Sample Position
Energy range : 0.75 - 1.9 Å
Energy resolution : 2 x 10-4
Photon flux : 2 x 1011@2.5 GeV, 450 mA, 1.0 Å
(0.2 x 0.2 mm slit)
Facilities in the Experimental Station
Detector : ADSC Quantum 315r
Detector size : 315 x 315 mm
Camera distance : 60 - 950 mm
Vertical offset : 0 - 150 mm
Cryocooling device : nitrogen gas flow around 95K
Fluorescence detector : Si-PIN photodiode
Workstation and Softwares
Computers
4 PC Workstations (Linux, CentOS6)
2 PC Windows (USB2.0, IEEE1394)
Softwares for image processing
HKL2000, DPS/Mosflm/Scala, XDS
Reference
to be published...
Contact Person
Naohiro Matsugaki (KEK-PF)
Phone : +81-298-64-5647
Fax : +81-298-64-2801
e-mail : naohiro.matsugaki@kek.jp
Other Information
Current photograph of BL-5A
Comparison with other PX beamlines in PF
User Manual for PX beamlines
PX beamlines at PF Japanese/ English
Beamtime schedules, beamline news, and so on
Structural Biology Research Center

Last modified: 2013-10-09